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1) DIBAL 2) H3O* H2CRO, (aq) (excess) SOCI2 TEA 1) CH3CH,ONa, (1 eq) CH;CH,OH H20, H2SO, heat 2) H3O* 1) CH3ONA, CH3OH 1) CH3ONA,

1) DIBAL 2) H3O* H2CRO, (aq) (excess) SOCI2 TEA 1) CH3CH,ONa, (1 eq) CH;CH,OH H20, H2SO, heat 2) H3O* 1) CH3ONA, CH3OH 1) CH3ONA, CH3OH OCH3 2) 2) Br 3) H3O*

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