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14. Build the 1H NMR for aspirin by drawing a peak for each of the unique hydrogens. Be sure to draw the peak at the
14. Build the 1H NMR for aspirin by drawing a peak for each of the unique hydrogens. Be sure to draw the peak at the correct chemical shift (this can be approximate value - you may use an NMR table) integration value, and splitting pattern for each unique hydrogen or set of unique hydrogens. Hint - be sure to consider both the inductive effect and resonance when determining the relative chemical shift values for the aromatic hydrogens. Label each peak to specify which hydrogen/set of hydrogens is responsible for the peak. - Analyze the 1H NMR spectrum obtained for the following transformation. Note: an aqueous workup was performed at the end of the reaction and the product the resultant solid was recrystallized from ethanol. cat.H3PO4 salicylic acid acetic anhydride acetylsalicylic acid acetic acid
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