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2 . 7 . Aniline is produced by the hydrogenation of nitrobenzene. A small amount of cyclo - hexylamine is produced as a by -

2.7. Aniline is produced by the hydrogenation of nitrobenzene. A small amount of cyclo-hexylamine is produced as
a by-product. The reactions are:
1.C2H5NO2+3H2C6H5NH2+2H2O
2.C6H5NO2+6H2C6H11NH2+2H2O
Nitrobenzene is fed to the reactor as a vapor, with three times the stoichiometric quantity of hydrogen. The
conversion of the nitrobenzene to all products is 96%, and the selectivity for aniline is 95%.
The unreacted hydrogen is separated from the reactor products and recycled to the reactor. A purge is taken
from the recycle stream to maintain the inerts in the recycle stream below 5%. The fresh hydrogen feed is 99.5%
pure, with the remainder being inerts. All percentages are molar.
For a feed rate of 100kmolh of nitrobenzene, calculate:
a. The fresh hydrogen feed
b. The purge rate required
c. The composition of the reactor outlet stream
Use Pro/ll to simulate the textbook problem 2.7. Assume feed
and hydrogen are available at 25F. Assume separation is done
with a flash drum at 50C. The conditions at the reactor is 200
C & 7KGCM2. Ignore pressure drops for this exercise.
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