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After troubleshooting. you discover the following: The column was running smoothly but not well. Reflux rate was too low, so it precluded significant fractionation. The
After troubleshooting. you discover the following:
The column was running smoothly but not well. Reflux rate was too low, so it precluded significant fractionation. The column pressure was KPa below design. Whenever the pressure reached KPa, the reboller pressure exceeded the hotoil pressure. The relatively lowboiling toluene then flowed into the hot oil and flashed. This generated a large volume of vapor that then backed hot oil out of the reboiler. The toluene vapors passed on into the main fractionator and flooded this tower. Only a small amount of vapor, but no liquid, was being produced from the reflux drum, which should have produced mainly liquid.
Explain three possible cause for the errors you observed.
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