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c. MeO2C OH OH 1. TrCl (1 eq) py, cat. DMAP 2. TBSOT 2,6-lutidine, CH2Cl2 3. LIBH4, THE C1 79% 4. Ph3P, 12 imidazole C2

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c. MeO2C OH OH 1. TrCl (1 eq) py, cat. DMAP 2. TBSOT 2,6-lutidine, CH2Cl2 3. LIBH4, THE C1 79% 4. Ph3P, 12 imidazole C2 89% c. MeO2C OH OH 1. TrCl (1 eq) py, cat. DMAP 2. TBSOT 2,6-lutidine, CH2Cl2 3. LIBH4, THE C1 79% 4. Ph3P, 12 imidazole C2 89%

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