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Figure 1 shows a simplified process and instrumentation diagram ( PI&D ) for a single unit of a fixed bed reactor for a catalytic steam

Figure 1 shows a simplified process and instrumentation diagram (PI&D) for a single unit of
a fixed bed reactor for a catalytic steam reforming process. The reactor is designed to produce
hydrogen from an acetic acid/steam reforming at the atmospheric pressure. Acetic acid
solution (acid/water) is fed by a pump, Pl which has an automatic control system. Nitrogen
functions as a carrier gas to support the fluid flow rate. The nitrogen flow is controlled by a
mass flow controller, MFC (control valve). The electrical furnace, Fl and pre-heater, PHl are
connected to a controller, Cl. The reaction is endothermic and it takes place after the acetic
acid solution is vaporized inside the reactor with the presence of nickel/cobalt catalyst. The
resulted products are channeled to a gas-liquid separator through a flanged piping system.
Figure 1: Schematic diagram of a fixed bed reactor with the feeding system
(a) Develop a HAZOP study for the reactor vessel based on the following requirements
listed in Table 1 below.
(b) List down all the actions required as per the HAZOP study in (a).
(c) Construct a new piping and instrumentation diagram (PID) of the system after
implementing the actions required listed in (b).
(d) Recommend two approaches which fall under the category of intensification and
attenuation (one approach for each) for making the system shown in Figure 1
inherently safer. Brief explanation on how the proposed approach can make the
system safer should be given.
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