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I could use some help answering the questions and i attached the spectral data 1) From the spectral data (H, IR, MS) you were given,
I could use some help answering the questions and i attached the spectral data
1) From the spectral data (H, IR, MS) you were given, identify the structure of your product. Explain why you chose your particular product based on the spectroscopic data. You will not receive full marks for determination of the unknown unless you explain why. 2) Based on your IR data, how would you rate the purity of your product? Are there any significant impurities, and if so, what is/are it/they? Det er 10400 Thu February 10, 2019 400 PM Analyst Date Teaching Thunday by 10.2002 403 101 100 95 90 85 80 75 70 %T 65 60 55 50 45 40 37 4000 1000 450 1500 2000 3000 3500 2500 cm-1 Teaching 09 Sample 009 By Teaching Date Thursday, February 10 2002 10:28 AM Fri Feb 18 D2.pdf @ee K 21 2 7 8 6 5 3 3 0 2 PPM LI 3X IN Figure 3. List of Potential Unknowns a) Potential Unknown Amines NH2 NH2 NH2 NH2 NH2 NH2 NH2 NH2 NH - NH2 NH2 Me CI NOZ 31.10 70.14 B.H (10.3 : 183.12 Me Br OME CI 12. 2 178.00 120.2 122 02 b) Potential Unknown Aldehydes CHO CHO CHO NO2 Br CHO CHO CHO La CHO 230.02 Me 58.08 -CHO 86.134 72.11 NM2 Br 185.02 86,10 CI 120.16 Br Figure 4. Generic Reductive Amination Procedure O HH + R-NH2 NaBH(OAc)3 R' R R I ZI Step by Step Solution
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