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Identify the species that are found in the test solution. N a 2 S C u S O 4 [ Z n ( N H

Identify the species that are found in the test solution.
Na2S
CuSO4
[Zn(NH3)4]2+
Na2SO4
CuS
NH3
SO42-
IncorrectProcedures
Experiment: Determine Limiting and Excess Reactants
Part 1: Prepare the Test Solution and Test Standards
Record all observations for this part in Table 13.1.
Take one 50mL beaker and one 50mL graduated cylinder from the Containers shelf. Measure 20.0mL6M ammonia
in the graduated cylinder, recording the exact volume at the meniscus, then transfer to the beaker. Put the used
graduated cylinder in the sink.
Take a new 50mL graduated cylinder from the Containers shelf. Take 0.4M zinc sulfate from the Materials shelf. Use
the graduated cylinder to measure 20.0mL, record the amount, then transfer to the beaker that contains the ammonia
solution. Put the used graduated cylinder in the sink. You have now prepared the test solution.
Take two test tubes and one 10mL graduated cylinder from the Containers shelf and place them on the workbench.
Double-click on the test tubes and label them "test tube standard 1" and "test tube standard 2".
Take 0.1 M copper(II) sulfate from the Materials shelf and measure 6.0mL into the graduated cylinder. Double-click on
the graduated cylinder and record the exact volume at the meniscus. Transfer the liquid to the test tube 1 and record the
color of the solution to reference later. Put the graduated cylinder in the sink.
Take a new 10mL graduated cylinder from the Containers shelf. Take 0.1M sodium sulfide from the Materials shelf
and measure 6.0mL into the graduated cylinder. Double-click on the graduated cylinder and record the exact volume at
the meniscus. Transfer the liquid to test tube 2 and record the color of the solution to reference later. Put the used
graduated cylinder in the sink.
Take a new 10mL graduated cylinder from the Containers shelf. Using the 10mL graduated cylinder, measure 2mL of
the test solution and pour 2mL into each of the two test tubes. Record any color changes and whether a precipitate
forms. The reaction should happen fairly quickly.
The first test tube shows what an excess of copper(II) sulfate looks like, and the second test tube shows what an excess
of sodium sulfide looks like. These are the standards against which to compare other samples. Double-click on each test
tube and label the tube for reference.
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