Question
Please help me out with this ASAP!!!!!!!!!!!!!!! Please create a pictorial flowchart out of the method below. Method 1. Accurately weigh 0.5 0.7 g of
Please help me out with this ASAP!!!!!!!!!!!!!!!
Please create a pictorial flowchart out of the method below.
Method
1. Accurately weigh 0.5 0.7 g of the sample into a 500 ml beaker. The sample must be
dried in an oven at 105 C for at least two (2) hours.
2. Add 200 250 ml of distilled water to dissolve the sample and then add 0.5 ml conc.
HCl.
3. Heat the solution to near boiling and then add 0.25M BaCl2 in a slow, continuous stream
from a burette while stirring the solution in the beaker constantly. Allow the precipitate
to settle at periodic intervals to determine if precipitation is complete. DO NOT
REMOVE THE GLASS ROD FROM THE BEAKER!! NB. Precipitation is complete when
BaCl2 added to the unstirred solution fails to produce any more precipitate.
4. When there is no indication of further precipitate being formed, add an extra 10% of the
volume of BaCl2 used to the contents of the beaker. Leave the glass rod in the beaker,
cover the beaker with a watch glass and digest on a steam bath until the supernatant
liquid is clear.
5. During this time, accurately weigh a covered porcelain crucible which has been heated
on a Bunsen burner for fifteen (15) minutes prior to being cooled in a desiccator.
6. Filter the contents of the beaker. ENSURE QUANTITATIVE TRANSFER OF ALL THE
PRECIPITATE FROM THE BEAKER TO THE FILTER PAPER.
7. Wash the precipitate with hot distilled water until no turbidity appears when a few ml
of washings, acidified with a few drops of dilute HNO3, are reacted with AgNO3. This is
the test for residual chloride.
8. Carefully fold the filter paper into a package enclosing the precipitate and place it into
the pre-weighed porcelain crucible.
9. Place the crucible in an inclined position on a pipe-clay triangle, with the cover slightly
displaced, over a Bunsen burner. Heat gently with a small flame until all the moisture is
driven off and the paper begins to smoke and char. Adjust the burner so that the paper
continues to char without catching fire. IF THE PAPER INFLAMES, COVER THE CRUCIBLE
TO SMOTHER THE FIRE, AND LOWER THE BUNSEN FLAME.
10. When the paper is completely carbonised and no more smoke is given off, gradually
raise the Bunsen flame enough to burn off the carbon completely. NB. The precipitate
should finally be white with no black particles. Allow the crucible and contents to cool.
11. Place the crucible in a vertical position in the pipe-clay triangle, and moisten the
precipitate with four (4) drops of dil. H2SO4, heat very gently until acid has fumed off.
Cover the crucible and heat to dull redness for fifteen (15) minutes.
12. Cool the covered crucible in a desiccator for one (1) hour and then weigh the crucible
and contents. Repeat the heating, cooling and weighing cycles until three successive
mass readings agree to within 0.5 mg.
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