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Prepare the buret. Place an empty waste beaker beneath the buret. Open the stopcock and rinse the buret with 5 - 1 0 mL of

Prepare the buret.
Place an empty waste beaker beneath the buret.
Open the stopcock and rinse the buret with 5-10 mL of deionized water.
Next, rinse the buret at least two times with 5-10mL of NaOH solution, collecting the waste in the beaker. (This step insures the buret is coated in the solution to be titrated.)
Close the stopcock.
Fill the buret to just past 0mL with NaOH solution.
Open the stopcock to release enough NaOH so the buret volume reads between 0-3 mL.
The collected waste solutions in the beaker may be poured down the drain.
Place the Erlenmeyer flask below the buret to begin titration.
Record the initial volume of NaOH below.
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