Answered step by step
Verified Expert Solution
Link Copied!

Question

1 Approved Answer

pulverized in a ball mill and the resulting powder was digested with various strong resulting solution was evaporated to dryness dissolved in dilute hydrochloric acid

image text in transcribed
image text in transcribed

pulverized in a ball mill and the resulting powder was digested with various strong resulting solution was evaporated to dryness dissolved in dilute hydrochloric acid and separated from interferents by ion exchange chromatography The resulting solution containing an unknown amount of Pd II was then diluted to 50 00 mL with pH 3 5 buffer Ten milliliter aliquots of this analyte solution were then transferred to six 50 mL volumetric flasks A standard solution was then prepared that was 1 00 10 5M in Pd 11 Volumes of the standard solution shown in the table were then pipetted into the volumetric flasks along with 10 00 mL of 0 01 M arsenazo III Each solution was then diluted to 50 00 mL and the absorbance of each solution was measured at 660 nm in 1 00 cm cells Volume Standard Solution mL 0 00 5 00 10 00 15 00 20 00 25 00 A660 0 216 0 338 0 471 0 596 0 764 0 850 a Enter the data into a spreadsheet and construct a standard additions plot of the data b Determine the slope and intercept of the line J G Sen Gupta Anal Chem 1967 39 18 DOI 10 1021 ac60245a029

Step by Step Solution

There are 3 Steps involved in it

Step: 1

blur-text-image

Get Instant Access to Expert-Tailored Solutions

See step-by-step solutions with expert insights and AI powered tools for academic success

Step: 2

blur-text-image

Step: 3

blur-text-image

Ace Your Homework with AI

Get the answers you need in no time with our AI-driven, step-by-step assistance

Get Started

Recommended Textbook for

Precalculus Mathematics For Calculus

Authors: James Stewart, Lothar Redlin, Saleem Watson

5th Edition

1111795355, 9781111795351

More Books

Students also viewed these Mathematics questions