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Suppose the following data is obtained from the proton NMR of the reaction at t = 90 min. Splitting Integration d J 4.81 0.76 0.36
Suppose the following data is obtained from the proton NMR of the reaction at t = 90 min. Splitting Integration d J 4.81 0.76 0.36 Shift (ppm) 1.1 1.4 2.0 2.4 3.2 3.6 3.9 4.0 4.7 4.9 5.0 S 5 brs brs dm brs d S 9 0.05 3.24 0.63 1. 603 0.12 1.603 0.12 0.253 OS a. Fill in the missing data in the table. Please show all work. For example, how did you determine the integration values? b. What is the mole percent of the intermediate 1? Please show your work. c. What is the mole percent of starting material? Please show your work. Hint for calculations: Which proton(s) do all 4 structures have in common? Use these for comparison.... Allu Arytones have citz in common. The Integrant 59 court Suppose the following data is obtained from the proton NMR of the reaction at t = 90 min. Splitting Integration d J 4.81 0.76 0.36 Shift (ppm) 1.1 1.4 2.0 2.4 3.2 3.6 3.9 4.0 4.7 4.9 5.0 S 5 brs brs dm brs d S 9 0.05 3.24 0.63 1. 603 0.12 1.603 0.12 0.253 OS a. Fill in the missing data in the table. Please show all work. For example, how did you determine the integration values? b. What is the mole percent of the intermediate 1? Please show your work. c. What is the mole percent of starting material? Please show your work. Hint for calculations: Which proton(s) do all 4 structures have in common? Use these for comparison.... Allu Arytones have citz in common. The Integrant 59 court
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