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The GC-MS data of the starting material, 4-tert-butylcyclohexanol, is provided below and the assigned 13CNMR APT (attached proton test) spectrum is provided on the subsequent
The GC-MS data of the starting material, 4-tert-butylcyclohexanol, is provided below and the assigned 13CNMR APT (attached proton test) spectrum is provided on the subsequent page. Although typical 13CNMR signal intensities are not quantitative due to how the NMR experiment is conducted, the qualitative intensities can be useful. Use the 13CNMR spectrum of the starting mixture to identify which isomer is present in the mixture in greater abundance. Using the relative abundances of the two isomers from the NMR data, identify the isomer responsible for GC traces 1 and 2. Use the GC peak integration data to calculate the relative amount of the major isomer to the minor isomer in the starting material in the format of X:1, whare 1 ie tha ralative amnnent of tha minne ienmer (2 nte) The GC-MS data of the starting material, 4-tert-butylcyclohexanol, is provided below and the assigned 13CNMR APT (attached proton test) spectrum is provided on the subsequent page. Although typical 13CNMR signal intensities are not quantitative due to how the NMR experiment is conducted, the qualitative intensities can be useful. Use the 13CNMR spectrum of the starting mixture to identify which isomer is present in the mixture in greater abundance. Using the relative abundances of the two isomers from the NMR data, identify the isomer responsible for GC traces 1 and 2. Use the GC peak integration data to calculate the relative amount of the major isomer to the minor isomer in the starting material in the format of X:1, whare 1 ie tha ralative amnnent of tha minne ienmer (2 nte)
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