An 8.13-g sample of an ant-control preparation was decomposed by wet-ashing with H2SO4 and HNO3. The As

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An 8.13-g sample of an ant-control preparation was decomposed by wet-ashing with H2SO4 and HNO3. The As in the residue was reduced to the trivalent state with hydrazine. After removal of the excess reducing agent, the As(III) required a 31.46-mL titration with 0.03142 M I2 in a faintly alkaline medium. Express the results of this analysis in terms of percentage of As2O3 in the original sample.
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Fundamentals of Analytical Chemistry

ISBN: 978-0495558286

9th edition

Authors: Douglas A. Skoog, Donald M. West, F. James Holler, Stanley R. Crouch

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