We are distilling a mixture that is (10.0 mathrm{~mol} %) methanol, (20.0 mathrm{~mol} %) ethanol, (30.0 mathrm{~mol}
Question:
We are distilling a mixture that is \(10.0 \mathrm{~mol} \%\) methanol, \(20.0 \mathrm{~mol} \%\) ethanol, \(30.0 \mathrm{~mol} \% \mathrm{n}\)-propanol, and \(40.0 \mathrm{~mol} \% \mathrm{n}\)-butanol. Methanol is most volatile and n-butanol is least volatile. The feed is a saturated liquid. We desire to recover \(98.0 \%\) of the ethanol in the distillate and \(97.0 \%\) of the n-propanol in the bottoms. The column has a total condenser and a partial reboiler. The feed rate is \(100.0 \mathrm{kmol} / \mathrm{h}\). Pressure is \(1.0 \mathrm{~atm} . \mathrm{L} / \mathrm{D}=3.0\).
1. The column is hottest at:
a. The condenser.
b. The feed plate.
c. The reboiler.
2. In the rectifying (enriching) section:
a. Liquid flow rate \(>\) vapor flow rate.
b. Liquid flow rate \(=\) vapor flow rate.
c. Liquid flow rate \(<\) vapor flow rate.
3. Comparing the stripping section to the rectifying section:
a. Liquid flow rate in stripping section \(>\) liquid flow rate in rectifying section.
b. Liquid flow rate in stripping section \(=\) liquid flow rate in rectifying section.
c. Liquid flow rate in stripping section \(<\) liquid flow rate in rectifying section.
4. The HK is:
a. Methanol.
b. Ethanol.
c. n-propanol.
d. n-butanol.
5. If you were going to do external mass balances around the column to find \(\mathrm{B}\) and \(\mathrm{D}\), the best assumption to make is:
a. All of the methanol and n-propanol are in distillate.
b. All of the methanol is in distillate, and all of the n-butanol is in bottoms.
c. All of the ethanol is in distillate, and all of the n-propanol is in bottoms.
d. All of the n-propanol and n-butanol are in bottoms.
Step by Step Answer:
Separation Process Engineering Includes Mass Transfer Analysis
ISBN: 9780137468041
5th Edition
Authors: Phillip Wankat