Question
Draw the correct structure from the MS, 1H NMR, 13C NMR, and IR data given below. Both of the peaks on the 1H NMR spectrum
Draw the correct structure from the MS, 1H NMR, 13C NMR, and IR data given below. Both of the peaks on the 1H NMR spectrum are doublets (J = 2.5 Hz) and the integration ratio is 1:1.
9 6,15 H Relative abundance 100- --09 --09 40- 20- 0.0+ 0.0 142 132 20 26 (13%) $14 120 5100% fully 40 52 (100%) m/z 60 (11%) 62 (4%) 60 09 to Chanical shift ppm) 80 87 (92%) 00 (30%) 100 9 # Chemical shit (ppm) % Transmittance 100 80- 60- 40- 20 132 0 4000 3500 3000 2500 2000 170 111 114 3198 II m 3039 2234 3127 1606 1500 Wavenumbers (cm-) 1000 Chemical shift p 500 20 SDBS, National Institute of Advanced Industrial Science and Technology
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Organic Chemistry
Authors: Graham Solomons, Craig Fryhle, Scott Snyder
11th edition
1118133579, 978-1118133576
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