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2 . 1 . Give an overview of a thermogravimetric analysis ( TGA ) and give the mechanisms of weight change during the analysis. 2

2.1. Give an overview of a thermogravimetric analysis (TGA) and give the mechanisms of weight change during the analysis.
2.2. Discuss the principles of the TGA technique. (6)
Figure 1: The TGA curves of (a) Polymer A,(b) Polymer B,(c) Polymer C.
2.3.
2.3.1. How many stages of weight loss are shown in Figure 1?
(1)
2.3.2. Give all the TGA stages which are undergone by Polymer A and include the temperature degradation.
(6)
2.3.3. Identify all the DSC peaks in Figure 2.
(4)
2.3.4. Define the DSC analysis.
(2)
4
Figure 2: DSC curve of the BaZrO3 nanoparticles.
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