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400 MHz NMR -7.032 7.011 ..0 10.5 1 1.94 10.0 -6.914 --6.903 -6.891 9.5 9.0 2 0.98 7.10 7.05 7.00 6.95 6.90 6.85 f1 (ppm)

400 MHz NMR -7.032 7.011 ..0 10.5 1 1.94 10.0 -6.914 --6.903 -6.891 9.5 9.0 2 0.98 7.10 7.05 7.00 6.95 6.90 6.85 f1 (ppm) 6E09- 8.5 8.0 6.828 3 1.92 6.80 CDC13 7.5 6.75 1.94 0.98 1.92 1.98 7.0 6.687 6.5 999 9 -6.666 4 6.70 6.65 1.98 6.0 5.5 f1 (ppm) 5.0 06E- 5 T 2.03 4.5 916 6 'T 2.99 4.0 3.5 3.0 -2.267 7 2.5 H 2.95 HCO OH 2.0 HN amine final product 1.5 1.0 0.5 C

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