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5 . 1 0 . - It is necessary to calculate the diameter at the base of a distillation column that separates ethylene glycol (

5.10.- It is necessary to calculate the diameter at the base of a distillation column that separates ethylene glycol (EG) and
diethylene glycol (DEG). The vapor and liquid flows in this area of the tower are 764 kmol/h and 968 kmol/h,
respectively. The bottom product has a composition of 98 mol% DEG and 2 mol% EG. The spine
operates at 1 bar and will use a 3" Intalox ceramic seat filler with a packing factor of 22 ft-1
. the fall
The maximum allowable pressure is 1.5 pumps of water per foot at water level. Obtain:
a) The allowable speed of the steam, in m/s
b) The diameter of the column, in m.
c) The liquid load, in m3
/(h m2
)
d) Comment on the results obtained: Is the selected column type appropriate? it is appropriate
The size of the filling chosen? Please reply.
DATA: The following data is found in the tower section considered:
- Temperature: 243.8C
- Pressure: 1 bar
- Molecular weights: 103.1 kg/kmol (vapor); 105.2(liquid)
- Densities: 2,455 kg/m3
(steam); 932.6kg/m3
(liquid)
- Surface tension: 26.65 dynes/cm
- Kinematic viscosity: 3,526 cSt (vapor); 0.1647 cSt (liquid).

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