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A process engineer aims to purify a feedstock containing 9 0 wt % active component ( A ) and 1 0 wt % of impurity
A process engineer aims to purify a feedstock containing wt active component A and wt of impurity I A preliminary separator is able to purify the feed to wt They build a new purification device capable of generating a product stream containing of the active substance A from its input stream and of the impurities from its input stream. An effluent stream out of the purifier carries the rest of A and impurities. They set up the purification process as shown in Figure The stream out of the separator is split equally in terms of mass flowrate into two channels. The first channel is sent directly to the purifier while the second stream is mixed with a recycle stream consisting of half the purifiers product stream. Both purifier I and purifier II are similar units. Assuming a basis of kghr of feedstock and steady state, a Develop a stream table and fill it with known flow rates and compositions b Find the flowrate of streams leaving the initial separator and the amounts of A and I in itc Calculate the flowrates of streams entering and leaving purifier I. d Calculate the flowrates of streams entering and leaving purifier IIe How does using a recycle stream affect the purity and recovery of component A e How does using a recycle stream affect the purity and recovery of component A Purity Amount of A in final product stream Total amount of substance in product stream Recovery Amount of A in final product stream Amount of A in feedstock Figure : Purification process Caution Remember that the streams leaving the purifier contain of A that was present in the input to the purifier and of I that was in the input to the purifier. Purity and recovery are to be determined based on the final streams leaving the purifier, ie after the recycle splitters.Problem points
A process engineer aims to purify a feedstock containing active component A and
of impurity I A preliminary separator is able to purify the feed to They build a new
purification device capable of generating a product stream containing of the active substance
A from its input stream and of the impurities from its input stream. An effluent stream out
of the purifier carries the rest of A and impurities. They set up the purification process as shown
in Figure The stream out of the separator is split equally in terms of mass flowrate into two
channels. The first channel is sent directly to the purifier while the second stream is mixed with
a recycle stream consisting of half the purifier's product stream. Both purifier I and purifier II are
similar units. Assuming a basis of of feedstock and steady state,
a Develop a stream table and fill it with known flow rates and compositions
b Find the flowrate of streams leaving the initial separator and the amounts of A and I in it
c Calculate the flowrates of streams entering and leaving purifier I.
d Calculate the flowrates of streams entering and leaving purifier II
e How does using a recycle stream affect the purity and recovery of component A
Purity
Recovery
Figure : Purification process
Caution Remember that the streams leaving the purifier contain of A that was present in the
input to the purifier and of I that was in the input to the purifier.
Purity and recovery are to be determined based on the final streams leaving the purifier, ie after the
recycle splitters.
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