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( c ) Shown below are a set of scanning electron micrographs of ZnO tetrapodal particles produced by flame transport synthesis, i . e .
c Shown below are a set of scanning electron micrographs of ZnO tetrapodal
particles produced by flame transport synthesis, ie the controlled combustion
of metallic Zn microparticles. Briefly, a slurry of zinc microparticles in poly
vinyl butyral and ethanol is loaded into crucible and placed in a muffle
furnace. The slurry is heated to for varied durations, with products
collected on substrates placed near the crucible.
i Describe the mechanism of formation of tetrapodal nano and
microparticles.
ii Suggest three other materials which may generate tetrapodal particles.
iii Describe a wetchemical method which may be used to produce
tetrapodal particles of one of the materials chosen in
iv One application envisaged for these ZnO tetrapods is in the formation of
hydrophobic materials. Why may these microstructures be suitable for
this purpose?
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