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3. Data Record numerical values with units and the correct number of significant figures. Table 2. Data mass of nutmeg volume of ether mass
3. Data Record numerical values with units and the correct number of significant figures. Table 2. Data mass of nutmeg volume of ether mass of dry, recrystallized Trimyristin literature melting range of Trimyristin 1.018 aml 0.055 56C-STC heating rate (ramp) in Cimin Tmelt Temelt AT (T-T) (10) 4. Calculate the % recovery of pure Trimyristin from nutmeg. Show your work X100% = (8) 6. Thought Questions. Briefly discuss. 20 54.4C 55.7C 1.3C 1.0785 (14) 5. Discuss the purity of your recrystallized Trimyristin: a) melting range in comparison to literature value, b) AT (Tsire-Taanis2.0 C is pure; AT 2.0C is not pure Show calculation a. What is the purpose of the Pasteur filter pipet? to separate the H0 from the solution. b. What is the meaning of "crude" product? and what does recrystallization do? unrefined product c. Why is the recrystallizing solution cooled in an ice bath? d. Nutmeg is approximately 18-30 % Trimyristin by mass. How does this percent compare with your results? 3. Data Record numerical values with units and the correct number of significant figures. Table 2. Data mass of nutmeg volume of ether mass of dry, recrystallized Trimyristin literature melting range of Trimyristin 1.018 aml 0.055 56C-STC heating rate (ramp) in Cimin Tmelt Temelt AT (T-T) (10) 4. Calculate the % recovery of pure Trimyristin from nutmeg. Show your work X100% = (8) 6. Thought Questions. Briefly discuss. 20 54.4C 55.7C 1.3C 1.0785 (14) 5. Discuss the purity of your recrystallized Trimyristin: a) melting range in comparison to literature value, b) AT (Tse-T)2.0 C is pure; AT 2.0 C is not pure Show calculation a. What is the purpose of the Pasteur filter pipet? to separate the H0 from the solution. b. What is the meaning of "crude" product? and what does recrystallization do? unrefined product c. Why is the recrystallizing solution cooled in an ice bath? d. Nutmeg is approximately 18-30% Trimyristin by mass. How does this percent compare with your results?
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