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*j. COH CH3 1. Na (> 2 eq), NH3 (1) t-BuOH, EtO 2. (Ph3P)3RhCl (cat.) H, toluene 3a. (CO)2Cl2 3b. EtOH J1 4. OsO4

*j. COH CH3 1. Na (> 2 eq), NH3 (1) t-BuOH, EtO 2. (Ph3P)3RhCl (cat.) H, toluene 3a. (CO)2Cl2 3b. EtOH J1 4. OsO4 (cat.), NalO4 (excess) HO, dioxane 5. Et3N, heat J2

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