explain in details the experipments that written in the following pictureParticle$/$crystal size were reduced further

by dissolving NTO into $N-$methyl pyrrolidone

$($NMP$)$ in a $65\frac{g}{100}g$ concentration at $90C.$

This solution was poured into ice water with

agitation and with ice being added to maintain

the temperature below $5C.$ Batch L$.$BC$-$III$-6$C$,$

shown in Figure $5,$ was made using this

procedure. This SEM photograph shows $50$ to

$100$ micron "clumps" that contain many $2$ to

$10$ micron crystals, but the crystals are ran$-$

domly packed and look like they contain a

large amount of voids.

N'TO dissolved in NMP and crashed into

ice water can produce spherical crystal growth

that is similar to spherical NQ produced at Los

Alamos. The crystal size produced with a $3$:$1$

ratio of $1_{2}O$:$NMP,$ shown in Figure $6,$ is very

small $($i$.$e$.,1-5$ microns$)$ and is in spheres rang.

ing from $10$ to $30$ microns in diameter. Indivi$-$

dual crystal size can be controlled by changing

the ratio of ice water to NMP:NTO solution.

Agglomerates containing a random arrange$-$

ment of small crystals can be obtained by adding

additional NMP:NTO solution to the combined

solutions after crystal formation has begun.

Small$-$crystal$-$size $($i$.$e$.,1-10$ micron$)$

spherical NTO produced by batch recrystal$-$

lization from NMP was pressed into $\frac{1}{2}$ inch

diameter pellets for plate dent comparison with

previously produced NTO. Plate$-$dent results

for Batch$-$III$-222,$ shown in Figure $7,$ were

$263\frac{k}{b}ar$ at $1\mathrm{.}764g^{c{m}^3}(91\mathrm{.}4\%$ TMD$)$ and

$257\frac{k}{b}ar$ at $1\mathrm{.}827\frac{g}{c}{m}^3(94\mathrm{.}7\%$ TMD$).$ Drop$-$