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Figure Q1 shows the Williams-Otto plant, named after T. I. Williams and R. E. Otto. Raw materials A and B are mixed in a CSTR

  1. Figure Q1 shows the Williams-Otto plant, named after T. I. Williams and R. E. Otto. Raw materials A and B are mixed in a CSTR and yield the following reactions:

A + B C C + B P + E P + C G

where P is the desired product, and E and G are undesired by-products. The three reactions have an overall exothermic effect and the CSTR is cooled with water. The effluent of the reactor is cooled with cooling water and enters a decanter, where the by-product G is removed. The remaining mixture enters a distillation column where the desired product P is removed as the top distillate stream. The bottom product contains unreacted A, B and by-products C and E. Part of it is removed while the rest is recycled back to the CSTR.

  1. The composition of distillate (Y1) and bottom (Y2) products from the distillation column are to be regulated to their desired set-points. The available manipulated variables are the reflux flow (U1) and steam flow rate (U2). The following input-output relationships for the distillation column have been determined experimentally:

Process transfer function A: G22 =(-19.4e-3s)/(14.4s+1)

Process transfer function B: G11 = (12.8e-s)/(16.7s+1)

Process transfer function C: G12 = (-18.9e-3s)/(21s+1)

Process transfer function D: G21 = (6.6e-7s)/(10.9s+1)

Your task is to select the pairings between controlled outputs and manipulated variables so that the resulting loops offer minimum steady-state interaction. If the best couplings still possess significant interaction between the control loops, design two decouplers that produce two non-interacting control loops.

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