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For monitoring the amide-forming reaction by TLC, the following procedure is recommended: Sample a few drops of the reaction mixture and transfer it into a
For monitoring the amide-forming reaction by TLC, the following procedure is recommended: Sample a few drops of the reaction mixture and transfer it into a test tube/vial containing about one millilitre of ethyl acetate and one millilitre of HCl 1M. Mix the biphasic solution vigorously before sampling some of the organic phase for your TLC plate. Why is such a procedure recommended?
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Introduction To Chemical Engineering Analysis Using Mathematica For Chemists Biotechnologists And Materials Scientists
Authors: Henry C. Foley
2nd Edition
0128200510, 978-0128200513
