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i need help with this its due in the next 20 minutes. thank you %Transmittance 101 Unknown C 100 99 98 97 96 95 94-
i need help with this its due in the next 20 minutes. thank you %Transmittance 101 Unknown C 100 99 98 97 96 95 94- 2986.18 3000 93 92 91- 90- 4000 3500 on Apr 18 09:59:09 2022 (GMT-07:00) ND PEAKS: Spectrum: Unknown C Region: 4000,00 400.00 Absolute threshold: 99.730 50 Sensitivity Peak list: Position: 847.40 Intensity: 99.261 Position: 938.37 Intensity: 99.593 Position: 1046.28 Intensity: 94,049 Position: 1096.73 Intensity: 99.337 Position: 1240.57 Intensity: 91.988 Position: 1373.43 Intensity 96.061 Position 1447 40 Intensity: 99.308 Position 1740.70 Intensity: 91.563 2000 Wavenumbers (cm-1) 2500 1740.70 1500 1447 40 1096,73 1373.43 1240 57 1046.28 1000 938.37 847.40 500 Position 2986.18 Intensity 99.663 Relative Intensity 100 80 60 40 20 MS-NU-0661 10 20 Source Temperature: Sample Temperature: RESERVOIR, 75 eV 30 220 C 150 C 40 50 Unknown C Mass of molecular ion = 86 60 70 80 90 m/z 100 - 1 1.1 * . elect vers Ivory le din IM 8. TE PROTE() 1 sovet FIT HT SE 16 YCIE let, pretoria LINE . BAR SUN . . 1 1 PIE. Atlas WIR B repetition DATA PROCESS FTP Yeti TREINAR *** add 12 10 10.17 Unknow, C Beta Cellected on Archive directorys Sample #trectory: Unknow20161105_2 Florile labe 1,01 Pale Sequence: PROTON (21) Solvant dels Data collected on: Nov 5 2018 Temp. 24. C/ 297.1 K ample 21, Operator: walaup Melax, delay 1.000 c ulse 45.0 degrees Ace.11nr 2.04 width 2012. HE se repetitions SERVE MS, 495.7870814 TA PROCESSING 4128 32768 tal time 3 a 15 sec 1.8 005-06 ww//A/60E[BA/2004/ THE 1.6 28.87 1.2 1.0 0.8 42.65 INDEX T E 4 S . CLARENCE 11 13 14 FREQUENCY PR 731.4 724.4 1.450 1.464 1.430 700. 1.420 703.1 1.407 1.311 647.8 4.20 $45.0 1.201 $32.7 1.366 $15.3 1.251 610.8 1.11 411.4 1.003 8.920 144.8 414.0 9.814 CALL HEIGHT 1.8 31.6 39.6 34.1 13.3 1:55# 0.4 7.2 24.3 1:00 37.8 11.8 5.7 8TH 1:59. ppm 111 THEY FR 101 3 3. I. 3.4 LY LY 15 14 elect 41 SIE URN RE POTIN ( TI PIR SHE title VE 4. SE STA BE Wy 2.6 2.4 add 2.8 3.0 3.8 3.5 3.2 3.4 20 10. 2011 Sample Unk Data Collected on nar-p-vars300 Archive strectory: ///visy/a Sample directory: DC20161105.01 fiaftler piasel,01 Pulse Sequence: CARBON (1) Solvent cdc13 Data collected on Nov 5 2010 Temp. 24.0C/287.1 E Sample 21, Operator: valeu Relax, delay 1.000 c Pulse 45.0 degrees Acg. Liar 1.04 width 31256. He 512 repetitions DESERVE C13, 125.8715010 Hitz DECOUPLE H, 438.7855003 MHZ Pover 42 continuously on VALT2-18 modulated DATA PROCESSING Lins broadening 8.5 He FT 120 65520 Total time 17 min 220 200 180 160 140 120 100 80 60 INDEX 40 FREQUENCY FPM $726. 17.30 1887.7 77.000 HEIGHT APN XP-X 2014.3 74.37 14.X 7783.8 41.40 10.3 030.1 34.007 111.8 1363.5 14.887 1717.3 18.878 M.A 20 ppm (1) Propose a structure for your unknown that is consistent with the IR, GC/MS, and 'H and 13C NMR spectra. (2) What are the major peaks in your IR spectrum. Assign these peaks to specific bond motions for functional groups that are present in your unknown. Note: only assign the major peaks in the 1500-4000 cm region. (3) What is the m/z value for the molecular ion for your unknown? What is the m/z value for the base peak in your unknown? Provide possible structures for ions that could be responsible for the major fragments (>25% intensity) in your mass spectrum. (4) Assign the peaks in your 'H NMR spectrum to the protons in your proposed structure. Explain how the chemical shifts, integrals and coupling in your spectrum are consistent with the proposed structure. (5) Assign the peaks in your 3C NMR spectrum to the carbons in your proposed structure. Explain how the chemical shifts in the spectrum are consistent with the proposed structure
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