Question
If I want to scale down this reaction to only use 10mg desthiobiotin NHS-ester, how would I do that? To create DBIA, to a solution
If I want to scale down this reaction to only use 10mg desthiobiotin NHS-ester, how would I do that?
To create DBIA, to a solution of desthiobiotin NHS-ester (100mg, 0.32mmol) in dichloromethane were added N,N-diisopropylethylamine (0.32mmol) and n-boc ethylenediamine (0.32mmol), and the reaction was stirred overnight at room temperature under a nitrogen atmosphere.
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Process Control A Practical Approach
Authors: Myke King
2nd Edition
1119157749, 978-1119157748
