Answered step by step
Verified Expert Solution
Link Copied!

Question

1 Approved Answer

In the pharmaceutical industry, distillation is utilized to exchange solvents in preparation for isolation of an active ingredient or intermediate. You are tasked with solvent

In the pharmaceutical industry, distillation is utilized to exchange solvents in preparation
for isolation of an active ingredient or intermediate. You are tasked with solvent swapping
an active ingredient from 1-Isobutanol (1-IBA) to Tetrahydrofuran (THF). All of the active
ingredients stay in the vapor phase and thus can be ignored in your analysis. Prior to
entering the distillation column, 325molh of 1-IBA and the active ingredient in the vapor
phase is mixed with 175molh of THF vapor to create a vapor feed of 500molh of a 35
mol%THF and 65mol%1-IBA at 3bar and 410K. This is fed to the 5 th tray of an 8-tray
distillation column equipped with a total condenser and a partial reboiler at 3 bar. The total
condenser produces saturated liquid. The bottoms fraction (BF) is 0.70 and the reflux ratio
(L0D) is 7.0. EMO can be assumed. Assume this mixture behaves ideally. Antoine's
Constants are given for log10 in bar and K.
a. Draw a process flow diagram.
b. Use a guess of xDTHF=0.94, solve for all unknowns for the Total Condenser and
Stage 1(Include a degree of freedom analysis for Total Condenser and Stage 1)
image text in transcribed

Step by Step Solution

There are 3 Steps involved in it

Step: 1

blur-text-image

Get Instant Access to Expert-Tailored Solutions

See step-by-step solutions with expert insights and AI powered tools for academic success

Step: 2

blur-text-image

Step: 3

blur-text-image

Ace Your Homework with AI

Get the answers you need in no time with our AI-driven, step-by-step assistance

Get Started

Recommended Textbook for

Methane Conversion Routes Status And Prospects

Authors: Vladimir Galvita, René Bos

1st Edition

1788014308, 978-1788014304

More Books

Students also viewed these Chemical Engineering questions

Question

List three differences between financial and managerial accounting.

Answered: 1 week ago

Question

8. discuss the concept of mindfulness.

Answered: 1 week ago

Question

friendliness and sincerity;

Answered: 1 week ago