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In the pharmaceutical industry, distillation is utilized to exchange solvents in preparation for isolation of an active ingredient or intermediate. You are tasked with solvent

In the pharmaceutical industry, distillation is utilized to exchange solvents in preparation
for isolation of an active ingredient or intermediate. You are tasked with solvent swapping
an active ingredient from 1-Isobutanol (1-IBA) to Tetrahydrofuran (THF). All of the active
ingredients stay in the vapor phase and thus can be ignored in your analysis. Prior to
entering the distillation column, 325molh of 1-IBA and the active ingredient in the vapor
phase is mixed with 175molh of THF vapor to create a vapor feed of 500molh of a 35
mol%THF and 65mol%1-IBA at 3bar and 410K. This is fed to the 5 th tray of an 8-tray
distillation column equipped with a total condenser and a partial reboiler at 3 bar. The total
condenser produces saturated liquid. The bottoms fraction (BF) is 0.70 and the reflux ratio
(L0D) is 7.0. EMO can be assumed. Assume this mixture behaves ideally. Antoine's
Constants are given for log10 in bar and K.
a. Draw a process flow diagram.
b. Use a guess of xDTHF=0.94, solve for all unknowns for the Total Condenser and
Stage 1(Include a degree of freedom analysis for Total Condenser and Stage 1)
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