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Moody [ 1 ] studied the efficiency of a GC separation of 2 - butanone on a dinonyl phthalate column. Evaluating plate height as a
Moody studied the efficiency of a GC separation of butanone on a dinonyl phthalate
column. Evaluating plate height as a function of flow rate gave a van Deemter equation for
which A is mm B is mmmLmin and C is mmminmL
a Using Microsoft Excel, plot a graph of H versus u for flow rates in the range of
mLmin Your graph must include curves due to the contributions of all the terms ie Curve for A B and C and the overall curve
b For what range of flow rates does each term in the Van Deemter equation have the
greatest effect?
c How much is the optimum flow rate for this column?
d How much is the height of a theoretical plate for the flow rate in part C
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