nformation: we had an experiment in which we did a synthesis of cyclohexene from cyclohexanol by elimination. We made a change in the desire to improve the product, and chose to double the amount of all the substances. write a theory part for the experiment.

the point of the experiment: How are the yield and purity of a product affected by different reaction conditions?

What we did: sand bath was heated to a stable temperature of approx. 140 C. 1.3 mL of cyclohexanol was added to the bulb flask, along with three drops of sulfuric acid, and some cooking stones.

the Hickman column was placed on the bulb flask, and the system was attached to a stand, approx. two cm deep in the sand. As the mixture began to boil, the bulb connector was covered in aluminum foil, to insulate heat, before a dropper was used to suck up the liquid on the side of the Hickman column. This liquid was transferred to a dram glass, and further, a small test tube with caustic soda. The mixture was then allowed to stand until the phases were separated. Then we sucked up the bottom phase, the water phase. The product that remained, in the uppermost phase, was the cyclohexene.

The experiment was then carried out again, where the volume of cyclohexanol, sulfuric acid and caustic soda was been doubled.

the mass of the cyclohexene during the first review was 0.496 grams, while the second 3.843.

Answer:

If we used bromide to test if it really was cyklohexene that was made, explain the purpose of this test, detailed. Which reaction type is it.