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OH 1. Add CHCl OH 1. Add NaOH (1 eq) 2. Mix 3. Allow Layers to Separate 2. Add NaHCO3 (1 eq) 3. Mix 4. Allow Layers to Separate HO CH2Cl2 Separate CH2Cl2 1. Add CHCl 2. Add HCI (1 eq) 3. Mix 4. Allow Layers to Separate HO CHCI HO Separate HO 1. Separate layers 2. Dry with NaSO4 3. Filter (decant) 4. Evaporate CH,CI, CHCI HO HO CHCl 1. Separate layers 2. Dry with NaSO 3. Filter (decant) 4. Evaporate CH.Cla CH2Cl2