Answered step by step
Verified Expert Solution
Link Copied!

Question

1 Approved Answer

Place 2-methyl-2-propanol (Alcohols folder) in the RBF and move a test tube sample to the clamp stand. Add chromic acid (H2CrO4) and record any changes

image text in transcribed
Place 2-methyl-2-propanol (Alcohols folder) in the RBF and move a test tube sample to the clamp stand. Add chromic acid (H2CrO4) and record any changes in the video window. Replace the test tube with a fresh sample, add ZnCl2, and observe any changes as the video progresses. Take the IR spectrum by dragging the cursor from the IR spectrometer to the RBF; record any significant signals. Collect the 13C spectrum by dragging the cursor from the NMR spectrometer to the RBF. Record how many signals show up, where they show (ppm values), and their relative intensities. Use your notes to match the statements below with your observations. When chromic acid was added the test tube contents became a blue/green colour because the alcohol was oxidized Two signals at a 1 to 3 ratio appeared in the carbon spectrum matching the C(CH3)3 part of the alcohol Adding zinc chloride caused the solution to become white and cloudy as the alcohol reacted The infrared spectrum showed the expected broad signal for the OH group at 3400 wavenumbers The orange colour of the chromic acid persisted when it was added to the tertiary alcohol The carbon spectrum shows 4 signals for the 4 carbons in the alcohol

Step by Step Solution

There are 3 Steps involved in it

Step: 1

blur-text-image

Get Instant Access to Expert-Tailored Solutions

See step-by-step solutions with expert insights and AI powered tools for academic success

Step: 2

blur-text-image

Step: 3

blur-text-image

Ace Your Homework with AI

Get the answers you need in no time with our AI-driven, step-by-step assistance

Get Started

Recommended Textbook for

Chemistry

Authors: Bryan Earl, Doug Wilford

3rd Edition

1444176447, 978-1444176445

More Books

Students also viewed these Chemistry questions

Question

Talk to me Sandra said before you change a thing.

Answered: 1 week ago