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please figure out the theoretical yield and % error the % error Mp is 33.2% Procide to trab an need flasswere lamk Round botten fiask
please figure out the theoretical yield and % error
the % error Mp is 33.2%
Procide to trab an need flasswere lamk Round botten fiask i 302m of AC etaminophen 0.5mLDD was combined Acetaminopten=0.309,Dmgo=1.4mL80%NaOH=0.237JIodoethare=0.332g heeded 200y of 80% vaot, 312m of I doed A Sir ba wass ad ded in to 10mL flasle with reactia. shir was places at 380 the cotar turned blue once Acetaminopten and Duso were combined positim reactia. - Hot plate was set at 190150C ( 141C) let heat up far 30 minuets - 10 minuessin in turned a tan Colar - almost 20 minuets in it turneda blackish/Tan Colar Aluminum blode tempture reached al' C retlux began "3o minuets" Loml of ice-cold wate wim test tude - places RBF in soml beake to reach room tempater Y Product was a little darker, temperthe jot a little too high between 10S110C Vaccum fiter was Set up 25mL filter flagk, filte pape saccun chander. Vaccum hose was set all te wq uf. Ilc Analysis AC= Acetaminophen P= Phenacetin my P= my prodect (crude e recrystalliz ec my producet was disolved in S- 6 drops of thyl acetate befar placed on +LC plate my froduct wars much darlar on ta tic plate Detinelt was ser at up. Paciced capiliary tube - 2-3mn of crude Solution tappedbottan of capilary tube rapp rate of 10C. Was set afte preheabed. temp for detil melt was set for 190C ranp rake of 0.5C. product melted at 133.2C135.20 Theoretical y ield =151.16g/mol309mgx00%=0.002042.04%Step by Step Solution
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