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Please write the answers to the following questions directly in your notebook. 1. Draw and label a detailed apparatus of the steam distillation apparatus used

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Please write the answers to the following questions directly in your notebook. 1. Draw and label a detailed apparatus of the steam distillation apparatus used for the synthesis of pinacolone (refer to the lab video). (6 pts) 2. After the steam distillation of the pinacolone product is complete, the distillation pot contains 12N2 hot H2SO4. How will you treat the 12NH2SO4 ? (3 pts) 3. Why is it important to dry the crude pinacolone product prior to the final semimicro distillation? (3 pts) 4. What visual criterion is to be used to assess whether the crude reaction product is dry prior to semimicro distillation? ( 3 pts) 5. Draw a detailed mechanism using curved arrow notation that leads to the formation of the major product for the pinacol rearrangement shown below. " H+ may be used for 3MHClO4 in your mechanism. (5 pts) 3MHClO4 >90%

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