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Provide a physical data table for all chemicals used in the following experiment. An example of the table is below. Here is an example of
Provide a physical data table for all chemicals used in the following experiment. An example of the table is below.
Here is an example of the table: mp F bp C Solubility Hazards density Chemical MW Name (g/mol) salicylic 138 157-159 acid - liver al, ace, eth damage Diels-Alder Reaction - A Greener Alternative This Diels-Alder reaction is performed in water and eliminates the requirement to prepare the starting material (thermal decomposition is required in the traditional approach). This approach takes advantage of the hydrophobic effect, which increases the reaction rate. As such, the reaction can be completed in an hour, even though the reagents are significantly less reactive than the traditional cyclopentadiene and 1,3-butadiene starting materials. 990.60 HO HO Experimental32 Caution: N-Methylmaleimide is corrosive and must be handled with care. Wear gloves and safety glasses at all times. 1. Weigh 65 mg of 9-anthracenemthanol into a 100 mL round bottom flask. 2. Add 50 mL of water and a magnetic stir bar. 3. Add 3 equivalents of N-methylmaleimide (0.104 g) to the reaction flask. 4. Fit the reaction flask with a reflux condenser and heat the reaction to reflux while stirring. 5. Monitor the progress of the reaction by TLC, eluting with 1:1 ethyl acetate/hexanes. Be sure to let all of the water evaporate before developing the TLC. 6. When the reaction is complete, after approximately one hour, allow the reaction to cool to room temperature, and then cool further in an ice-water bath. 7. Collect the product by vacuum filtration. 8. Record the weight, melting point, and IR spectrum in a KBr pellet of your final productStep by Step Solution
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