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R . D Snee ( Experiment with a large number of variables, in Experiments in industry: Design, analysis and interpretation of results, by R

R. D Snee ("Experiment with a large number of variables", in Experiments in industry: Design,
analysis and interpretation of results, by R. D. Snee, L. B Hare, and J. B. Trout, Editors, ASQC,
1985) describes an experiment in which a 25-1 design with I=ABCDE was used to investigate the
effects of five factors on the color of chemical product. The factors are A: solvent/reactant, B:
catalyst/reactant, C: temperature, D: reactant purity, E: reactant pH. The responses obtained were
follows:
e=-0,06,d=6,85
a=2,55 ade =5,50
b=-2,68 bde =3,48
abe =1,60 abd =5,75
c=2,06 cde =5,25
ace =1,22 acd =4,40
bce =-2,09bcd=4,32
abc=1,93 abcde =4,00
a. Prepare a normal probability plot of the effects. Which effect seem active?
b. Calculate the residuals. Construct a normal probability plot of the residual and plot the residual
versus the fitted values. Comment on the plots.
c. If any factors are negligible, collapse the 25-1 design into a full factorial in the active factors.
Comment on the resulting design, and interpret the results.
answerd with minitab !!
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