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RESULTS: Volume and molarity of P b ( N O 3 ) 2 solution Volume and molarity of H 2 S O 4 solution 1

RESULTS:
Volume and molarity of Pb(NO3)2 solution
Volume and molarity of H2SO4 solution
15mL&0.5M
15mL&0.5M
Mass of crucible
Mass of crucible + plumbum sulphate
(1st Weigh - before heating)
Mass of crucible + plumbum sulphate
(2nd Weigh - after heating)
Mass of crucible + plumbum sulphate
(3rd Weigh)
Mass of plumbum sulphate precipitates formed
(1 mark)
QUESTIONS:
Write the balanced equation for the reaction.
(1 mark)
Assume that the experiment is conducted ideally with both reactants fully reacted. Determine which reactant is the limiting and excess, if any.
(4 marks)
Based on the same ideal condition set in Question 2, will the mass of plumbum sulphate increases if you use 20mLPb(NO3)2 solution? Why?
(2 marks)
Based on your calculation in Question 2, how much plumbum sulphate you should actually get? Explain one (1) possible reason why the mass that you calculated is different than the collected one.
(3 marks)
What is the percentage yield for plumbum sulphate in this experiment?
(1 mark)
If you use Mg(NO3)2 instead of Pb(NO3)2, do you think the experiment may proceed accordingly using the same lab procedure? Explain. (Hint: Check their solubility)
(3 marks)
The precipitate is required to be rinsed several times before filtration. Briefly discuss the reason(s) rinsing is required and whether the timing of rinsing (before or during filtration) makes any difference to the obtained precipitate.
(2 marks)
Discuss the pros and cons of burning the filter paper to obtain the precipitate versus drying it in the drying cabinet.
(2 marks)
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