Answered step by step
Verified Expert Solution
Link Copied!

Question

1 Approved Answer

Synthesized cinnamic acid using the following reaction The conditions were chosen in such a way that the malonic acid (starting material) was limiting and benzaldehyde

Synthesized cinnamic acid using the following reaction The conditions were chosen in such a way that the malonic acid (starting material) was limiting and benzaldehyde was in excess. During the workup (extraction) the following steps were done.The reaction mixture was in ethyl acetate was washed with 1.0 M HCl (3x)It was extracted with NaHCO3 (3x)The NaHCO3 was acidified to pH 1 and extracted with ethyl acetate (3x)The ethyl acetate (from previous step) was washed with brine (1x)The ethyl acetate was dried over MgSO4, filtered and evaporated Explain each step and discuss which compound is in which layer per step.
student submitted image, transcription available

H .

Step by Step Solution

3.37 Rating (156 Votes )

There are 3 Steps involved in it

Step: 1

Introduction The synthesis of cinnamic acid involves several steps and the workup process plays a crucial role in isolating the desired product while ... blur-text-image

Get Instant Access to Expert-Tailored Solutions

See step-by-step solutions with expert insights and AI powered tools for academic success

Step: 2

blur-text-image

Step: 3

blur-text-image

Ace Your Homework with AI

Get the answers you need in no time with our AI-driven, step-by-step assistance

Get Started

Recommended Textbook for

Organic Chemistry

Authors: John McMurry

7 Edition

978-0495112587, 0495112585

More Books

Students also viewed these Chemical Engineering questions

Question

=+c) Do you find evidence of a seasonal effect? Explain.

Answered: 1 week ago