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The expected melting point range of the Diels Alder product is 237-239 o C. We did not purify the product in the Diels Alder reaction,

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The expected melting point range of the Diels Alder product is 237-239oC. We did not purify the product in the Diels Alder reaction, would you expect the melting point range to be higher or lower than the ideal mp. How can you fix the difference in mp? Please answer them all

DIenophile mass: N-methylmaleimide 0.11g

Dienee mass: Anthracene-9-methanol 0.08g

Mass of Anthracene-N-Methylmaleimide = 0.090g (product)

MP of the Anthracene-N-Methylmaleimide = 218-219 degree Celsius

Diels Alder Lab Questions 1. Which reagent is the limiting reagent in the Diels Alder reaction and why? 2. The expected melting point range of the Diels Alder product is 237-239C. We did not purify the product in the Diels Alder reaction, would you expect the melting point range to be higher or lower than the ideal me. How can you fix the difference in me? 3. Why is the Diels Alder reaction a 4+2 cycloaddition ? 4. What happens to the excess N-methyl maleimide? How many equivalents of N-methyl maleimide did we use in the Diels Alder reaction? 5.What would be the theoretical yield of the product in grams. Show calculations. 6. What kind of diene and dienophile should one use in the Diels Alder reaction? (talk about EWG and EWG) 7. What is the product of the following reaction? COOCH3 HEAT COOCH3

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