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The gas phase oxidation of o-xylene to phthalic anhydride is given below: CH10 +302 -> C3H103 + 3H2O This reaction is extremely exothermic. It is
The gas phase oxidation of o-xylene to phthalic anhydride is given below: CH10 +302 -> C3H103 + 3H2O This reaction is extremely exothermic. It is carried out in PFR tube bundles with molten salt circulating as the heat transfer fluid. The o-xylene is mixed with air before entering the PFR. The reaction rate is limited by maintaining a low concentration of hydrocarbon in the feed, i.e., the mole fraction of o-xylene is generally less than 2% Under these conditions, the large excess of oxygen leads to a pseudo-first order rate expression, i.e., the reaction rate is first order in o-xylene and roughly zero order in oxygen. The reactor operates at 1.0 atm. The PFR has a length of 1.5m and a radius of 0.0125m. The following data is also provided (Assume all species have the same heat capacity, Cp): km = 2.0822 sec-1 (1) Tm = 625K (1) T. = 625 K (1) EA = 1.3636 x 109K R (1) Cp = 32 J mol-1 K-1 (1) Ua= 59.68 JL-'-'K-1 (1) AHR= -1.284 x 10 J mol-1 (1) FA = 0.0018 mol sec-1 (1) FB= 0.0194 mol sec-1 (1) -1 Fi= 0.0730 mol sec (1) Part 1 As a warm up, calculate the temperature and o-xylene composition profile as a function of reactor volume for for feed temperatures of 615K, 620K, 625K, and 630K. Plot the Temperature vs. Volume profiles for all conditions in a single 2D plot. Interpret the trends you observe. Part 2 Now calculate the temperature and o-xylene composition profile as a function of reactor volume for feed temperatures ranging from 400 to 700K in 10 degree increments. Plot the Temperature vs. Volume profiles for all feed temperatures in a single 3D plot (e.g., a contour plot, heat map, surface plot, etc.)
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