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You have an 82.7 ppm Mn stock solution used to determine the amount of Mn in steel via standard additions. There is 1.0032 g of
You have an 82.7 ppm Mn stock solution used to determine the amount of Mn in steel via standard additions. There is 1.0032 g of steel dissolved in acid and diluted to 250 mL in a class A volumetric flask. Solutions were prepared according to the following table, diluted to 50 mL and the absorbance values were reported. Determine the percent Mn in the steel sample.
Sample | Steel solution (mL) | H3PO4 (mL) | Standard Mn solution (mL) | KIO4 (g) | Absorbance |
1 (blank) | 20.0 | 5.0 | 0 | 0 | ----- |
2 | 20.0 | 5.0 | 0 | 0.4 | 0.0786 |
3 | 20.0 | 5.0 | 1.0 | 0.4 | 0.1540 |
4 | 20.0 | 5.0 | 2.0 | 0.4 | 0.2264 |
5 | 20.0 | 5.0 | 3.0 | 0.4 | 0.3004 |
6 | 20.0 | 5.0 | 4.0 | 0.4 | 0.3785 |
7 | 20.0 | 5.0 | 5.0 | 0.4 | 0.4483 |
Determine the percent Mn in the steel sample.
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