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(a) C.H.Br (3 pts) 13C NMR Spectrum OC - 115.7 16.30 33 150 140 130 120 110 100 GE RE 'H NMR Spectrum 3.02 1.001.01

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(a) C.H.Br (3 pts) 13C NMR Spectrum OC - 115.7 16.30 33 150 140 130 120 110 100 GE RE 'H NMR Spectrum 3.02 1.001.01 1 1.5 10 270 0.5 25 45 40 35 3.0 SS 75 09 70 65 HSQC Spectrum 10 Red 30 40 Blue : SO -- 60 (dd) F1 ( 70 -80 90 -100 Blue Blue 110 120 2.5 20 3.0 4.5 4.0 5.0 3.5 PPM HH-COSY Spectrum: -25 -20 -- 2.5 -3.0 11 (ppm) - 35 4.0 -4.5 . -5.0 2.5 2.0 3.0 4.5 4.0 3.5 PPM 5.0 7 of 11 (a) C.H.Br (3 pts) 13C NMR Spectrum OC - 115.7 16.30 33 150 140 130 120 110 100 GE RE 'H NMR Spectrum 3.02 1.001.01 1 1.5 10 270 0.5 25 45 40 35 3.0 SS 75 09 70 65 HSQC Spectrum 10 Red 30 40 Blue : SO -- 60 (dd) F1 ( 70 -80 90 -100 Blue Blue 110 120 2.5 20 3.0 4.5 4.0 5.0 3.5 PPM HH-COSY Spectrum: -25 -20 -- 2.5 -3.0 11 (ppm) - 35 4.0 -4.5 . -5.0 2.5 2.0 3.0 4.5 4.0 3.5 PPM 5.0 7 of 11

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