Answered step by step
Verified Expert Solution
Link Copied!

Question

1 Approved Answer

In the pharmaceutical industry, distillation is utilized to exchange solvents in preparation for isolation of an active ingredient or intermediate. You are tasked with solvent

In the pharmaceutical industry, distillation is utilized to exchange solvents in preparation for isolation of an active ingredient or intermediate. You are tasked with solvent swapping an active ingredient from 1-Isobutanol (1-IBA) to Tetrahydrofuran (THF). All of the active ingredient stays in the vapor phase and thus can be ignored in your analysis. Prior to entering the distillation column, 325molh of 1- IBA and the active ingredient in the vapor phase is mixed with 175molh of THF vapor to create a vapor feed of 500molh of a 35mol% THF and 65mol%1-IBA at 3 bar and 410K. This is fed to the 5 th tray of an 8-tray distillation column equipped with a total condenser and a partial reboiler at 3 bar. The total condenser produces a saturated liquid. The bottoms fraction (BF) is 0.70 and the reflux ratio (L0D) is 7.0. EMO can be assumed. Assume this mixture behaves ideally. Antoine's Constants are given for log10 in bar and K.
A,B,C
THF 4.121181202.942-46.818
1-IBA 4.400621260.453-92.588
a. Draw a process flow diagram
b. Use a guess of xDTHF=0.94, solve for all unknowns for the Total Condenser and Stage 1(Include a degree of freedom analysis for Total Condenser and Stage 1)
image text in transcribed

Step by Step Solution

There are 3 Steps involved in it

Step: 1

blur-text-image

Get Instant Access to Expert-Tailored Solutions

See step-by-step solutions with expert insights and AI powered tools for academic success

Step: 2

blur-text-image_2

Step: 3

blur-text-image_3

Ace Your Homework with AI

Get the answers you need in no time with our AI-driven, step-by-step assistance

Get Started

Recommended Textbook for

Introduction To Chemical Engineering Tools For Today And Tomorrow

Authors: Kenneth A. Solen, John N. Harb

5th Edition

0470885726, 978-0470885727

More Books

Students also viewed these Chemical Engineering questions

Question

5. Identify three characteristics of the dialectical approach.

Answered: 1 week ago

Question

7. Identify six intercultural communication dialectics.

Answered: 1 week ago