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With the reference to the figure below, electron microscopy indicates that the grain size of the milled powder ( a ) is in the range
With the reference to the figure below, electron microscopy indicates that the grain size of the milled powder a is in the range of and that of the consolidated powder b is and above. On the basis that the increased broadening in a arises solely as a result of the fine crystallite size, show that the Xray data is consistent with the microscopical data.
Fig. Diffractometer charts radiation, : showing the first three reflections for a steel specimen Fe bcc in a the annealed condition and b after heavy surface abrasion giving broadened and shifted Xray diffraction peaks which arise from residual stresses on the microand macroscale and a reduction in crystallite size. Data by courtesy of Mr D G Wright.
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